{Rh(P(C₆H₂(OCH₃)3)3)2(CO)}⁽¹⁺⁾*BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2(CO)}(BF₄)

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Chemical Name:{Rh(P(C₆H₂(OCH₃)3)3)2(CO)}⁽¹⁺⁾*BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2(CO)}(BF₄)
CAS No.:134821-08-2
Molecular Formula:BF₄*C₅₅H₆₆O₁₉P₂Rh
Molecular Weight:1282.78
Hs Code.:

{Rh(P(C<sub>6</sub>H<sub>2</sub>(OCH<sub>3</sub>)3)3)2(CO)}<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>={Rh(P(C<sub>6</sub>H<sub>2</sub>(OCH<sub>3</sub>)3)3)2(CO)}(BF<sub>4</sub>)

Synonyms:{Rh(P(C₆H₂(OCH₃)3)3)2(CO)}⁽¹⁺⁾*BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2(CO)}(BF₄)

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Chemical Property of {Rh(P(C₆H₂(OCH₃)3)3)2(CO)}⁽¹⁺⁾*BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2(CO)}(BF₄)

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Technology Process of {Rh(P(C₆H₂(OCH₃)3)3)2(CO)}⁽¹⁺⁾*BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2(CO)}(BF₄)

There total 4 articles about {Rh(P(C₆H₂(OCH₃)3)3)2(CO)}⁽¹⁺⁾*BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2(CO)}(BF₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 14104-20-2
silver tetrafluoroborate

: 91608-15-0
tris(2,4,6-trimethoxyphenyl)phosphine

: 134821-08-2
{Rh(P(C₆H₂(OCH₃)3)3)2(CO)}⁽¹⁺⁾*BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2(CO)}(BF₄)

Guidance literature:: With CO; In tetrahydrofuran; (Ar), stirred for 5 min, filtered, phosphine containing CO-saturated THF added dropwise over several minutes at 0°C, stirred for 1 h; precipitated by diethyl ether, filtered in air, recrystd. from CH2Cl2/THF by reduction of volume and slow addn. of diethyl ether;

Reference yield: 60.0%

: 1277-43-6,78206-33-4
cobaltocene

: Rh(P(C₆H₂(OCH₃)3)3)2⁽²⁺⁾*2BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2}(BF₄)2

: 134821-08-2
{Rh(P(C₆H₂(OCH₃)3)3)2(CO)}⁽¹⁺⁾*BF₄^(1-)={Rh(P(C₆H₂(OCH₃)3)3)2(CO)}(BF₄)

Guidance literature:: With CO; In dichloromethane; (CO), stirred for 20 min; diethyl ether added, cooled to -5°C for 24 h, filtered, washed with diethyl ether, recrystd. from CH2Cl2/THF by reduction of volume and slow addn. of diethyl ether, filtered in air, washed with diethyl ether, dried in vac., elem. anal.;