(Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Base Information

Chemical Name:(Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione
CAS No.:120063-29-8
Molecular Formula:C₁₆H₂₀N₂O₅
Molecular Weight:320.345
Hs Code.:

Synonyms:(Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Suppliers and Price of (Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

There total 4 articles about (Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 120040-37-1
(Z)-4-(4-methoxyphenylmethyl)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

: 120063-29-8
(Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Guidance literature:: With sulfuric acid; In trifluoroacetic acid; at 25 ℃; for 12h;
DOI:10.1248/cpb.36.2607

Reference yield:

: 113296-74-5
(Z)-1-acetyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

: 120063-29-8
(Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride / 1.) DMF, 0 deg C, 30 min; 2.) DMF, 25 deg C, 12 h

2: 50.2 percent / hydrazine hydrate / dimethylformamide / 1 h / 25 °C

3: 1.) sodium hydride / 1.) DMF, 0 deg C, 30 min; 2.) DMF, 25 deg C, 1 h

4: 69 percent / H₂SO₄ / trifluoroacetic acid / 12 h / 25 °C

With sulfuric acid; sodium hydride; hydrazine hydrate; In N,N-dimethyl-formamide; trifluoroacetic acid;
DOI:10.1248/cpb.36.2607

Reference yield:

: 120040-36-0
(Z)-4-(4-methoxyphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

: 120063-29-8
(Z)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) DMF, 0 deg C, 30 min; 2.) DMF, 25 deg C, 1 h

2: 69 percent / H₂SO₄ / trifluoroacetic acid / 12 h / 25 °C

With sulfuric acid; sodium hydride; In trifluoroacetic acid;
DOI:10.1248/cpb.36.2607