2-chloro-6-cyclohexylbenzoyl chloride

Base Information

Chemical Name:2-chloro-6-cyclohexylbenzoyl chloride
CAS No.:1562995-60-1
Molecular Formula:C₁₃H₁₄Cl₂O
Molecular Weight:257.16
Hs Code.:

Synonyms:2-chloro-6-cyclohexylbenzoyl chloride

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Chemical Property of 2-chloro-6-cyclohexylbenzoyl chloride

Chemical Property:

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Technology Process of 2-chloro-6-cyclohexylbenzoyl chloride

There total 4 articles about 2-chloro-6-cyclohexylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 685892-23-3
methyl 2-acetyl-6-chlorobenzoate

: 1562995-60-1
2-chloro-6-cyclohexylbenzoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,4-dioxane / 3 h / 90 °C / Inert atmosphere

2: palladium on activated charcoal; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr

3: water; sodium hydroxide / methanol / 48 h / 80 °C

4: thionyl chloride / 24 h / Reflux; Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; thionyl chloride; palladium on activated charcoal; water; hydrogen; sodium carbonate; sodium hydroxide; In 1,4-dioxane; methanol; water; ethyl acetate;

Reference yield:

: 93224-85-2
2-bromo-6-chlorobenzoic acid

: 1562995-60-1
2-chloro-6-cyclohexylbenzoyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide monohydrate / tetrahydrofuran / 1 h / 25 °C

1.2: 21 h / 85 °C

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,4-dioxane / 3 h / 90 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr

4.1: water; sodium hydroxide / methanol / 48 h / 80 °C

5.1: thionyl chloride / 24 h / Reflux; Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; thionyl chloride; lithium hydroxide monohydrate; palladium on activated charcoal; water; hydrogen; sodium carbonate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; water; ethyl acetate;

Reference yield:

: 1562995-58-7
methyl 2-chloro-6-cyclohexylbenzoate

: 1562995-60-1
2-chloro-6-cyclohexylbenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / methanol / 48 h / 80 °C

2: thionyl chloride / 24 h / Reflux; Inert atmosphere

With thionyl chloride; water; sodium hydroxide; In methanol;