3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester

Base Information

Chemical Name:3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester
CAS No.:125687-07-2
Molecular Formula:C₂₃H₂₆ClNO₂
Molecular Weight:383.918
Hs Code.:

Synonyms:3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester

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Chemical Property of 3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester

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Technology Process of 3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester

There total 5 articles about 3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54491-23-5
2,2-dimethyl-4-hydroxyhexanoic acid γ-lactone

: 125687-07-2
3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 5 N NaOH, 2.) NaOCl solution / 2.) RuO₂*2H₂O / 1.) water, 1 h, ambient temperature, 2.) below 10 deg C

2: conc. H₂SO₄ / Heating

3: conc. H₂SO₄ / ethanol / Heating

With sodium hydroxide; sodium hypochlorite; sulfuric acid; ruthenium(IV) oxide; In ethanol;
DOI:10.1021/jo00296a063

Reference yield:

: 15118-53-3
2,2-dimethyl-4-oxohexanoic acid

: 125687-07-2
3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: conc. H₂SO₄ / Heating

2: conc. H₂SO₄ / ethanol / Heating

With sulfuric acid; In ethanol;
DOI:10.1021/jo00296a063

Reference yield:

: 59-88-1
phenylhydrazine hydrochloride

: 125687-07-2
3-[1-(4-Chloro-benzyl)-3-methyl-1H-indol-2-yl]-2,2-dimethyl-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / 1.) triethylamine, 2.) HCl gas / toluene / 6 h / Heating

2: conc. H₂SO₄ / ethanol / Heating

With hydrogenchloride; sulfuric acid; triethylamine; In ethanol; toluene;
DOI:10.1021/jo00296a063