(2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat

Base Information

• Chemical Name: (2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat
• CAS No.: 77441-41-9
• Molecular Formula: C₅H₁₃O₂S*C₆H₂N₃O₉S
• Molecular Weight: 429.386

Synonyms:(2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat

Chemical Property of (2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat

Chemical Property:

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Technology Process of (2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat

There total 1 articles about (2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-trinitrobenzensulfonate (2508-19-2) + (E)-<2-(Dimethylamino)vinyl>ethylmethylsulfonium-tetrafluoroborat → (2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat (77441-41-9)

Guidance literature:

With hydrogenchloride; Yield given. Multistep reaction; 1.) RT, 30 min; 2.) water;

Reference yield: 97.0%

methanol (67-56-1) + (2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat (77441-41-9) → (2-Hydroxy-2-methoxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat (77441-43-1)

Guidance literature:

Reference yield: 95.0%

(2.2-Dihydroxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat (77441-41-9) + trimethyl orthoformate (149-73-5) → (2.2-Dimethoxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat (77441-44-2)

Guidance literature:

With trinitrobenzenesulfonic acid; In methanol; 1.) 60 deg C, 3 h; 2.) RT, 10 h;

upstream raw materials:

2,4,6-trinitrobenzensulfonate

Downstream raw materials:

(2-Hydroxy-2-methoxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat

(2.2-Dimethoxyethyl)ethylmethylsulfonium-2.4.6-trinitrobenzolsulfonat

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