dimethyl((1-phenylvinyl)oxy)silyl acetate

Base Information

Chemical Name:dimethyl((1-phenylvinyl)oxy)silyl acetate
CAS No.:1638623-59-2
Molecular Formula:C₁₂H₁₆O₃Si
Molecular Weight:236.343
Hs Code.:

Synonyms:dimethyl((1-phenylvinyl)oxy)silyl acetate

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Chemical Property of dimethyl((1-phenylvinyl)oxy)silyl acetate

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Technology Process of dimethyl((1-phenylvinyl)oxy)silyl acetate

There total 3 articles about dimethyl((1-phenylvinyl)oxy)silyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₃ClOSi

: 64-19-7,77671-22-8
acetic acid

: 1638623-59-2
dimethyl((1-phenylvinyl)oxy)silyl acetate

Guidance literature:: With triethylamine; In acetonitrile; at 0 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201400405

Reference yield:

: 136559-54-1
N,N-diethyl-1,1-dimethyl-1-((1-phenylvinyl)oxy)silanamine

: 1638623-59-2
dimethyl((1-phenylvinyl)oxy)silyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere; Schlenk technique

2: triethylamine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

With triethylamine; acetyl chloride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/anie.201400405

Reference yield:

: 98-86-2
acetophenone

: 1638623-59-2
dimethyl((1-phenylvinyl)oxy)silyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide; triethylamine / acetonitrile / 4 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: triethylamine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

With triethylamine; sodium iodide; In acetonitrile;
DOI:10.1002/anie.201400405