(4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride

Base Information

Chemical Name:(4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride
CAS No.:928211-77-2
Molecular Formula:C₂₁H₂₇ClN₄O₅S*ClH
Molecular Weight:519.449
Hs Code.:

Synonyms:(4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride

Chemical Property:

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Technology Process of (4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride

There total 7 articles about (4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 928211-76-1
(4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-nitro-benzylamide

: 928211-77-2
(4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride

Guidance literature:: (4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-nitro-benzylamide; With hydrogen; palladium 10% on activated carbon; In methanol;

With hydrogenchloride; In 1,4-dioxane; methanol; at 0 ℃; for 1.5h;

Reference yield:

: 928211-73-8
(4-chlorobenzylsulfonyl)-D-Ser(O-tBu)-Cl

: 928211-77-2
(4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane

1.2: 20 °C / Cooling with ice

2.1: methyl-phenyl-thioether; trifluoroacetic acid / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol

3.2: 1.5 h / 0 °C

With methyl-phenyl-thioether; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In methanol; dichloromethane;

Reference yield:

: 928211-71-6
N-Me-Ala-4-nitrobenzylamide hydrochloride

: 928211-77-2
(4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-amino-benzylamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane

1.2: 20 °C / Cooling with ice

2.1: methyl-phenyl-thioether; trifluoroacetic acid / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol

3.2: 1.5 h / 0 °C

With methyl-phenyl-thioether; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In methanol; dichloromethane;