C₉H₇FO₂

Base Information

Chemical Name:C₉H₇FO₂
CAS No.:1225870-67-6
Molecular Formula:C₉H₇FO₂
Molecular Weight:166.152
Hs Code.:

C<sub>9</sub>H<sub>7</sub>FO<sub>2</sub>

Synonyms:C₉H₇FO₂

Suppliers and Price of C₉H₇FO₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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price

Total 1 raw suppliers

Chemical Property of C₉H₇FO₂

Chemical Property:

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Safty Information:

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Technology Process of C₉H₇FO₂

There total 7 articles about C₉H₇FO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 124-38-9,18923-20-1
carbon dioxide

: 766-49-4
(2-fluorophenyl)acetylene

: 1225870-67-6
C₉H₇FO₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 12h; under 15001.5 Torr; regioselective reaction;
DOI:10.1021/acscatal.0c01687

Reference yield:

: 57486-67-6
methyl o-fluorophenylacetate

: 1225870-67-6
C₉H₇FO₂

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / toluene / 12 h / 80 °C

2: potassium hydroxide / water; tetrahydrofuran / 2 h / Reflux

With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; potassium hydroxide; In tetrahydrofuran; water; toluene;
DOI:10.1021/acs.orglett.8b00982

Reference yield:

: 79477-86-4
2-fluorophenylglyoxylic acid

: 1225870-67-6
C₉H₇FO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: 0.17 h / Molecular sieve; Inert atmosphere; Cooling with ice

1.2: 20 °C / Inert atmosphere; Cooling with ice

1.3: 0.5 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

3.1: lithium hydroxide / tetrahydrofuran; water / 80 °C

With potassium hexamethylsilazane; lithium hydroxide; In tetrahydrofuran; water;
DOI:10.1021/acs.orglett.6b00748