C₄₈H₆₀N₄O₁₂Si

Base Information

Chemical Name:C₄₈H₆₀N₄O₁₂Si
CAS No.:274683-45-3
Molecular Formula:C₄₈H₆₀N₄O₁₂Si
Molecular Weight:913.11
Hs Code.:

C<sub>48</sub>H<sub>60</sub>N<sub>4</sub>O<sub>12</sub>Si

Synonyms:C₄₈H₆₀N₄O₁₂Si

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Chemical Property of C₄₈H₆₀N₄O₁₂Si

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Technology Process of C₄₈H₆₀N₄O₁₂Si

There total 7 articles about C₄₈H₆₀N₄O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 274683-45-3
C₄₈H₆₀N₄O₁₂Si

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / imidazole / tetrahydrofuran

2: 89 percent / acetic acid; water

3: NBS; 2,6-lutidine; 4 Angstroem molecular sieve / CH₂Cl₂

4: acetic acid; water

5: 30 percent / H₂O; acetonitrile / UV-irradiation

6: 55 percent / pyridine

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; N-Bromosuccinimide; 4 A molecular sieve; water; acetic acid; In tetrahydrofuran; dichloromethane; water; acetonitrile; 1: silylation / 2: Hydrolysis / 3: Condensation / 4: Hydrolysis / 5: Cyclization / 6: Substitution;
DOI:10.1016/S0040-4039(00)00127-1

Reference yield:

: 129185-32-6
5'-O-(4,4'-dimethoxytrityl)-3'-O-(methylthiomethyl)thymidine

: 274683-45-3
C₄₈H₆₀N₄O₁₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: NBS; 2,6-lutidine; 4 Angstroem molecular sieve / CH₂Cl₂

2: acetic acid; water

3: 30 percent / H₂O; acetonitrile / UV-irradiation

4: 55 percent / pyridine

With pyridine; 2,6-dimethylpyridine; N-Bromosuccinimide; 4 A molecular sieve; water; acetic acid; In dichloromethane; water; acetonitrile; 1: Condensation / 2: Hydrolysis / 3: Cyclization / 4: Substitution;
DOI:10.1016/S0040-4039(00)00127-1

Reference yield:

: 80971-33-1
5'-O-(4,4'-dimethoxytrityl)-3'-O-(t-butyldimethylsilyl)-2'-deoxythymidine

: 274683-45-3
C₄₈H₆₀N₄O₁₂Si

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / acetic acid; water

2: NBS; 2,6-lutidine; 4 Angstroem molecular sieve / CH₂Cl₂

3: acetic acid; water

4: 30 percent / H₂O; acetonitrile / UV-irradiation

5: 55 percent / pyridine

With pyridine; 2,6-dimethylpyridine; N-Bromosuccinimide; 4 A molecular sieve; water; acetic acid; In dichloromethane; water; acetonitrile; 1: Hydrolysis / 2: Condensation / 3: Hydrolysis / 4: Cyclization / 5: Substitution;
DOI:10.1016/S0040-4039(00)00127-1