methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate

Base Information

Chemical Name:methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate
CAS No.:1180491-83-1
Molecular Formula:C₂₈H₂₆O₈
Molecular Weight:490.51
Hs Code.:

Synonyms:methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate

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Chemical Property of methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate

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Technology Process of methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate

There total 5 articles about methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 5798-75-4
Ethyl 4-bromobenzoate

: 1180491-75-1
methyl 3-(3,5-dimethoxyphenyl)-6-methoxybenzofuran-4-carboxylate

: 1180491-83-1
methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate

: 1180491-78-4
dimethyl 3,3'-bis(3,5-dimethoxyphenyl)-6,6'-dimethoxy-2,2'-bibenzofuran-4,4'-dicarboxylate

Guidance literature:: With potassium acetate; palladium diacetate; In 2,4-dichlorophenoxyacetic acid dimethylamine; at 80 ℃; for 16h;
DOI:10.1039/b901911a

Reference yield: 51.0%

: 1613483-85-4
methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-(ethoxycarbonyl)phenyl)-2-oxoethoxy)-5-methoxybenzoate

: 1180491-83-1
methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 130 ℃;
DOI:10.1021/jo500885w

Reference yield:

: 19520-74-2
3-hydroxy-5-methoxy-benzoic acid methyl ester

: 1180491-83-1
methyl 3-(3,5-dimethoxyphenyl)-2-(4-(ethoxycarbonyl)phenyl)-6-methoxybenzofuran-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 2 h / 80 °C

2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 120 °C

3: toluene-4-sulfonic acid / toluene / 130 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; acetone; toluene; mineral oil;
DOI:10.1021/jo500885w