N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester

Base Information

Chemical Name:N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester
CAS No.:1262413-96-6
Molecular Formula:C₂₀H₂₃N₃O₄
Molecular Weight:369.42
Hs Code.:

Synonyms:N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester

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Chemical Property of N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester

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Technology Process of N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester

There total 5 articles about N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5398-44-7
2,6-dichloropyridine-4-carboxylic acid

: 1262413-96-6
N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide; methanol / water / 4 h / 34 - 70 °C

1.2: 20 °C

2.1: sulfuric acid / methanol / 24 h / Reflux

3.1: bis[1,2-bis(diphenylphosphino)ferrocene]-palladium⁽⁰⁾ / water; tetrahydrofuran / 3 h / 85 °C / Inert atmosphere

4.1: hydrogenchloride; sodium hydroxide / ethanol; water / 0.5 h / 90 °C

5.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 2 h / 20 °C

With hydrogenchloride; methanol; sulfuric acid; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; bis[1,2-bis(diphenylphosphino)ferrocene]-palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water;

Reference yield:

: 42521-10-8
2-chloro-6-methoxyisonicotinic acid methyl ester

: 1262413-96-6
N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: bis[1,2-bis(diphenylphosphino)ferrocene]-palladium⁽⁰⁾ / water; tetrahydrofuran / 3 h / 85 °C / Inert atmosphere

2: hydrogenchloride; sodium hydroxide / ethanol; water / 0.5 h / 90 °C

3: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 2 h / 20 °C

With hydrogenchloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; bis[1,2-bis(diphenylphosphino)ferrocene]-palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; water;

Reference yield:

: 1122089-67-1
2-cyclopentyl-6-methoxypyridine-4-carboxylic acid

: 5331-43-1
N-benzyloxycarbonyl-hydrazine

: 1262413-96-6
N'-(2-cyclopentyl-6-methoxypyridine-4-carbonyl)hydrazinecarboxylic acid benzyl ester

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;