1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

Base Information

Chemical Name:1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione
CAS No.:113296-73-4
Molecular Formula:C₁₉H₂₄N₂O₇
Molecular Weight:392.409
Hs Code.:

Synonyms:1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

Chemical Property:

Purity/Quality:

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Technology Process of 1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

There total 5 articles about 1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 108-24-7
acetic anhydride

: 113296-72-3
1-acetyl-3-(2,4,5-trimethoxy-3-methylphenyl)methyl-2,5-piperazinedione

: 113296-73-4
1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

Guidance literature:: at 110 ℃; for 4h;
DOI:10.1248/cpb.35.2525

Reference yield:

: 3027-05-2
N,N'-diacetylpiperazin-2,5-dione

: 113296-73-4
1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / potassium tert-butoxide / 2-methyl-propan-2-ol; dimethylformamide / 24 h / Ambient temperature

2: 97 percent / H₂ / 10percent palladium on carbon / ethanol; dimethylformamide / 4 h / 760 Torr

3: 83 percent / 4 h / 110 °C

With potassium tert-butylate; hydrogen; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1248/cpb.35.2525

Reference yield:

: 60059-09-8
2,4,5-trimethoxy-3-methylbenzaldehyde

: 113296-73-4
1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / potassium tert-butoxide / 2-methyl-propan-2-ol; dimethylformamide / 24 h / Ambient temperature

2: 97 percent / H₂ / 10percent palladium on carbon / ethanol; dimethylformamide / 4 h / 760 Torr

3: 83 percent / 4 h / 110 °C

With potassium tert-butylate; hydrogen; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1248/cpb.35.2525