(acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle

Base Information

Chemical Name:(acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle
CAS No.:87093-75-2
Molecular Formula:C₁₉H₂₀N₂O₆S
Molecular Weight:404.444
Hs Code.:

Synonyms:(acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle

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Chemical Property of (acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle

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Technology Process of (acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle

There total 8 articles about (acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67-56-1
methanol

: 87093-74-1
(acetyl-5 6H-thiazine-1,3 yl-2)-2 phtalimido-2 propionate de methyle

: 87093-75-2
(acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle

Guidance literature:: With triethylamine;
DOI:10.1016/S0040-4039(00)87330-X

Reference yield: 80.0%

: 78-94-4,25038-87-3
methyl vinyl ketone

: 87093-73-0
(N,N-dimethylaminoethylene)amino-3 methly-2 o-methoxycarbonylbenzamido-2 thioxo-3 propionate de methyle

: 87093-75-2
(acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle

Guidance literature:: With hydroquinone; In benzene; for 72h; Heating;

Reference yield:

: 83344-06-3
N-Phthaloyl cyano-2 glycinate de methyle

: 87093-75-2
(acetyl-5 6H-thiazine-1,3 yl-2)-2 o-methoxycarbonylbenzamido-2 propionate de methyle

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / potassium carbonate / acetone / 1 h / Heating

2: 79 percent / triethylamine / 1 h / Heating

3: 80 percent / hydrogen sulfide, pyridine, triethylamine / 4 h / Ambient temperature

4: 87 percent / CHCl₃ / 2 h / Ambient temperature

5: 80 percent / hydroquinone / benzene / 72 h / Heating

With pyridine; hydrogen sulfide; potassium carbonate; triethylamine; hydroquinone; In chloroform; acetone; benzene;