2,5-Dimethyl-3-nitrobenzaldehyde

Base Information

Chemical Name:2,5-Dimethyl-3-nitrobenzaldehyde
CAS No.:69022-52-2
Molecular Formula:C9H9 N O3
Molecular Weight:179.17
Hs Code.:2913000090
DSSTox Substance ID:DTXSID20510999
Wikidata:Q72470982
Mol file:69022-52-2.mol

Synonyms:2,5-DIMETHYL-3-NITROBENZALDEHYDE;69022-52-2;Benzaldehyde, 2,5-dimethyl-3-nitro-;SCHEMBL7103655;DTXSID20510999;SNIIADHYLUSXJJ-UHFFFAOYSA-N;2,5-dimethyl-3-nitro-benzaldehyde

Suppliers and Price of 2,5-Dimethyl-3-nitrobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2,5-Dimethyl-3-nitrobenzaldehyde 95+%
1g
$ 842.00

Alichem
2,5-Dimethyl-3-nitrobenzaldehyde
1g
$ 1490.00

Alichem
2,5-Dimethyl-3-nitrobenzaldehyde
500mg
$ 863.90

Alichem
2,5-Dimethyl-3-nitrobenzaldehyde
250mg
$ 504.00

Total 7 raw suppliers

Chemical Property of 2,5-Dimethyl-3-nitrobenzaldehyde

Chemical Property:

PSA：62.89000
LogP:2.54730
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:179.058243149
Heavy Atom Count:13
Complexity:211

Purity/Quality:

99% ^*data from raw suppliers

2,5-Dimethyl-3-nitrobenzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)[N+](=O)[O-])C)C=O

Technology Process of 2,5-Dimethyl-3-nitrobenzaldehyde

There total 5 articles about 2,5-Dimethyl-3-nitrobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.4%

: 69022-52-2
dimethyl-2,5 nitro-3 benzaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h;

Reference yield: 53.0%

: 18102-22-2
1-(chloromethyl)-2,5-dimethyl-3-nitrobenzene

: 69022-52-2
dimethyl-2,5 nitro-3 benzaldehyde

Guidance literature:: With hydrogenchloride; hexamethylenetetramine; acetic acid; In water; for 2.5h; Heating;
DOI:10.1021/jo01299a028

Reference yield: 27.0%

: 7790-94-5
chlorosulfonic acid

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 89-58-7
mononitro-p-xylene

: 1202389-18-1
2,5-dimethyl-4-nitrobenzaldehyde

: 69022-52-2
dimethyl-2,5 nitro-3 benzaldehyde

Guidance literature:: chlorosulfonic acid; formaldehyd; mononitro-p-xylene; With sodium chloride; at 10 - 20 ℃; for 16h;

With hexamethylenetetramine; acetic acid; In water; for 2h; Reflux;

With hydrogenchloride; In water; for 0.333333h; Overall yield = 35 %; Overall yield = 4.2 g; Reflux;
DOI:10.1039/c5ob02482j