1H-Imidazole-4,5-dicarboxylic acid, 2-phenyl-, 4,5-dimethyl ester

Base Information

Chemical Name:1H-Imidazole-4,5-dicarboxylic acid, 2-phenyl-, 4,5-dimethyl ester
CAS No.:52122-98-2
Molecular Formula:C13H12 N2 O4
Molecular Weight:260.249
Hs Code.:
Mol file:52122-98-2.mol

Synonyms:1H-Imidazole-4,5-dicarboxylicacid, 2-phenyl-, dimethyl ester (9CI); 4,5-Bis(methoxycarbonyl)-2-phenylimidazole;Dimethyl 2-phenylimidazole-4,5-dicarboxylate

Suppliers and Price of 1H-Imidazole-4,5-dicarboxylic acid, 2-phenyl-, 4,5-dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1H-Imidazole-4,5-dicarboxylic acid, 2-phenyl-, 4,5-dimethyl ester

Chemical Property:

PSA：81.28000
LogP:1.64990

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole-4,5-dicarboxylic acid, 2-phenyl-, 4,5-dimethyl ester

There total 8 articles about 1H-Imidazole-4,5-dicarboxylic acid, 2-phenyl-, 4,5-dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67-56-1
methanol

: 1097966-68-1
5-(methoxycarbonyl)-2-phenyl-1H-imidazole-4-carboxylic acid

: 52122-98-2
dimethyl 2-phenyl-1H-imidazole-4,5-dicarboxylate

Guidance literature:: With sulfuric acid; for 50h; Reflux;
DOI:10.1002/jhet.5570450611

Reference yield: 79.0%

: 67-56-1
methanol

: 888-60-8
2-phenyl-1H-imidazole-4,5-dicarboxylic acid

: 52122-98-2
dimethyl 2-phenyl-1H-imidazole-4,5-dicarboxylate

Guidance literature:: methanol; 2-phenyl-1H-imidazole-4,5-dicarboxylic acid; With sulfuric acid; for 20h; Heating / reflux;

With sodium hydroxide; In methanol; at 0 ℃; pH=~ 7;

Reference yield: 62.0%

: 154546-41-5
(Z)-2-Benzylamino-but-2-enedioic acid dimethyl ester

: 52122-98-2
dimethyl 2-phenyl-1H-imidazole-4,5-dicarboxylate

Guidance literature:: With trimethylsilylazide; eosin y; In acetonitrile; at 20 ℃; Inert atmosphere; Schlenk technique; Irradiation; Green chemistry;
DOI:10.1021/acs.orglett.0c03269