2H-Imidazole-2-thione, 1,3-dihydro-4-methyl-1-[(4-nitrophenyl)amino]-5-phenyl-

Base Information

• Chemical Name: 2H-Imidazole-2-thione, 1,3-dihydro-4-methyl-1-[(4-nitrophenyl)amino]-5-phenyl-
• CAS No.: 191349-29-8
• Molecular Formula: C16H14 N4 O2 S
• Molecular Weight: 0
• Mol file: 191349-29-8.mol

Synonyms:2H-Imidazole-2-thione, 1,3-dihydro-4-methyl-1-[(4-nitrophenyl)amino]-5-phenyl-

Chemical Property of 2H-Imidazole-2-thione, 1,3-dihydro-4-methyl-1-[(4-nitrophenyl)amino]-5-phenyl-

Chemical Property:

• PSA: 110.66000
• LogP: 4.90070

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2H-Imidazole-2-thione, 1,3-dihydro-4-methyl-1-[(4-nitrophenyl)amino]-5-phenyl-

There total 1 articles about 2H-Imidazole-2-thione, 1,3-dihydro-4-methyl-1-[(4-nitrophenyl)amino]-5-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium thioacyanate (333-20-0) + 2-bromo-1-phenyl-1-propanone (2114-00-3) + 4-nitrophenylhydrazone (100-16-3) → 2,3-dihydro-4-methyl-1-(4-nitrophenylamino)-5-phenyl-1H-imidazole-2-thione (191349-29-8)

Guidance literature:

Yield given. Multistep reaction; 1) DMF, RT, 1 h, 2) DMF, 5 h;

DOI:10.3987/com-96-7715

Reference yield: 74.0%

2,3-dihydro-4-methyl-1-(4-nitrophenylamino)-5-phenyl-1H-imidazole-2-thione (191349-29-8) → 4-methyl-1-(4-nitrophenylamino)-5-phenyl-1H-imidazole

Guidance literature:

With dihydrogen peroxide; In acetic acid; for 0.166667h; Ambient temperature;

DOI:10.3987/com-98-8116

Reference yield: 40.0%

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose (6974-32-9) + 2,3-dihydro-4-methyl-1-(4-nitrophenylamino)-5-phenyl-1H-imidazole-2-thione (191349-29-8) → 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4-methyl-1-(4'-nitrophenylamino)-5-phenyl-1H-imidazole-2-thione

Guidance literature:

With iodine; at 160 ℃; for 0.333333h;

DOI:10.1081/NCN-120021429

upstream raw materials:

potassium thioacyanate

2-bromo-1-phenyl-1-propanone

4-nitrophenylhydrazone

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