2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine

Base Information

• Chemical Name: 2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine
• CAS No.: 161808-42-0
• Molecular Formula: C₂₇H₂₇Cl₃N₄O₃
• Molecular Weight: 561.895
• Mol file: 161808-42-0.mol

Synonyms:2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine

Chemical Property of 2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine

There total 1 articles about 2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

triethylentetramine (112-24-3) + 5-chlorosalicyclaldehyde (635-93-8) → 2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine (161808-42-0)

Guidance literature:

In methanol; at 0 - 65 ℃; for 3h;

DOI:10.1039/c7ce01269a

Reference yield: 54.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + 2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine (161808-42-0) + dysprosium(III) chloride hexahydrate → 2C27H24Cl3N4O3(3-)*2Dy(3+)*2C4H8O

Guidance literature:

tetrahydrofuran; 2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine; With triethylamine; In methanol; for 2h;

dysprosium(III) chloride hexahydrate; In methanol; for 3h;

DOI:10.1039/c9ra08754k

Reference yield: 51.0%

2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine (161808-42-0) + dysprosium(III) chloride hexahydrate + acetone (67-64-1) → 2C27H24Cl3N4O3(3-)*2Dy(3+)*2C3H6O

Guidance literature:

2-(2'-hydroxy-5'-chlorophenyl)-1,3-bis[3'-aza-4′-(2''-hydroxy-5''-chlorophenyl)prop-4'-en-1'-yl]-1,3-imidazolidine; acetone; With triethylamine; In methanol; for 2h;

dysprosium(III) chloride hexahydrate; In methanol; for 3h;

DOI:10.1039/c9ra08754k

upstream raw materials:

triethylentetramine

5-chlorosalicyclaldehyde