1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride

Base Information

• Chemical Name: 1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride
• CAS No.: 60095-53-6
• Molecular Formula: C₂₂H₁₆F₂N₂*2Cl
• Molecular Weight: 417.285
• Mol file: 60095-53-6.mol

Synonyms:1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride

Chemical Property of 1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride

There total 2 articles about 1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1′-bis(2,4-dinitrophenyl)-[4,4′-bipyridine]-1,1′-diium chloride (41168-79-0) + 4-fluoroaniline (371-40-4) → 1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride (60095-53-6)

Guidance literature:

In ethanol; water; at 80 ℃; for 24h;

DOI:10.1246/bcsj.64.321

Reference yield:

4,4'-bipyridine (553-26-4) → 1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride (60095-53-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / acetonitrile / 72 h / Heating

2: ethanol; H₂O / 24 h / 80 °C

In ethanol; water; acetonitrile;

DOI:10.1246/bcsj.64.321

Reference yield: 86.0%

2C19H18N8O2(2-)*Co(3+)*C12H28N(1+) + 1,1'-bis(4-fluorophenyl)-4,4'-bipyridinium dichloride (60095-53-6) → 4C19H18N8O2(2-)*2Co(3+)*C22H16F2N2(2+)

Guidance literature:

In methanol; at 50 ℃; for 3h;

upstream raw materials:

1,1′-bis(2,4-dinitrophenyl)-[4,4′-bipyridine]-1,1′-diium chloride

4-fluoroaniline

4,4'-bipyridine