3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ⁴,10λ⁴-ditellura-tricyclo[10.2.2.2^5,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene

Base Information

• Chemical Name: 3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ⁴,10λ⁴-ditellura-tricyclo[10.2.2.2^5,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene
• CAS No.: 130484-11-6
• Molecular Formula: C₄₀H₃₆O₈Te₂
• Molecular Weight: 899.921

Synonyms:3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ⁴,10λ⁴-ditellura-tricyclo[10.2.2.2^5,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene

Chemical Property of 3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ⁴,10λ⁴-ditellura-tricyclo[10.2.2.2^5,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene

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Technology Process of 3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ⁴,10λ⁴-ditellura-tricyclo[10.2.2.2^5,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene

There total 3 articles about 3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ⁴,10λ⁴-ditellura-tricyclo[10.2.2.2^5,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

Te,Te-di(p-methoxyphenyl)-N-(p-tolylsulfonyl)tellurimide (62486-35-5) + hydroquinone (123-31-9,8027-02-9) → bis(4-methoxyphenyl)telluride (4456-34-2) + 3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ4,10λ4-ditellura-tricyclo[10.2.2.25,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene (130484-11-6) + toluene-4-sulfonamide (70-55-3) + p-benzoquinone (106-51-4)

Guidance literature:

In chloroform; for 0.25h; Heating;

Reference yield:

di(p-methoxyphenyl)tellurium dichloride (4456-36-4) → 3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ4,10λ4-ditellura-tricyclo[10.2.2.25,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene (130484-11-6)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol; toluene / Ambient temperature

2: CHCl₃ / Heating

In methanol; chloroform; toluene;

Reference yield:

C16H20O4Te (104690-02-0) + hydroquinone (123-31-9,8027-02-9) → 3,3,10,10-Tetrakis-(4-methoxy-phenyl)-2,4,9,11-tetraoxa-3λ4,10λ4-ditellura-tricyclo[10.2.2.25,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene (130484-11-6)

Guidance literature:

In chloroform; Yield given; Heating;

upstream raw materials:

Te,Te-di(p-methoxyphenyl)-N-(p-tolylsulfonyl)tellurimide

hydroquinone

C₁₆H₂₀O₄Te

di(p-methoxyphenyl)tellurium dichloride

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