N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester

Base Information

Chemical Name:N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester
CAS No.:1330059-20-5
Molecular Formula:C₃₁H₃₃NO₅S
Molecular Weight:531.673
Hs Code.:

Synonyms:N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester

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Chemical Property of N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester

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Technology Process of N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester

There total 1 articles about N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 957753-00-3
(9H-fluoren-9-yl)methanethiol

: 13574-13-5
Boc-Glu(OBzl)-OH

: 1330059-20-5
N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ja2065158

Reference yield: 76.0%

: 1330059-20-5
N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester

: 623-33-6
glycine ethyl ester hydrochloride

: 72917-81-8
N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamylglycine ethyl ester

Guidance literature:: N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester; With piperidine; In N,N-dimethyl-formamide;

With hydrogenchloride;

glycine ethyl ester hydrochloride; With N,O-bis-(trimethylsilyl)-acetamide; In tetrahydrofuran; at 20 ℃; for 8h;

Reference yield:

: 1330059-20-5
N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester

: 1186060-38-7
Boc-L-Glu(OBn)-SH

Guidance literature:: N-α-tert-butoxycarbonyl-γ-benzyl ester L-glutamine 9-fluorenylmethyl thioester; With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

With hydrogenchloride; In N,N-dimethyl-formamide;
DOI:10.1021/ja2065158