methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?

Base Information

Chemical Name:methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?
CAS No.:1428847-44-2
Molecular Formula:C₁₅H₂₀BrNO₅S
Molecular Weight:406.298
Hs Code.:

Synonyms:methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?

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Chemical Property of methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?

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Technology Process of methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?

There total 4 articles about methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate? which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1428847-43-1
methyl 3-(cyclopropylmethoxy)-4-(N-(2-hydroxyethyl)methylsulfonamido)benzoate?

: 1428847-44-2
methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃; for 2h;

Reference yield: 77.0%

: 1239278-73-9
3-cyclopropylmethoxy-4-methanesulfonylaminobenzoic acid methyl ester

: 603-35-0
triphenylphosphine

: 1428847-44-2
methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?

Guidance literature:: With carbon tetrabromide; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 1239278-74-0
3-cyclopropylmethoxy-4-(N-tert-butoxycarbonyl-N-methanesulfonyl)aminobenzoic acid methyl ester

: 1428847-44-2
methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / dichloromethane / 72 h / 20 °C

2: potassium carbonate / acetonitrile / 12 h / 110 °C / Microwave irradiation

3: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 20 °C

With hydrogenchloride; carbon tetrabromide; potassium carbonate; triphenylphosphine; In dichloromethane; acetonitrile;