lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Base Information

Chemical Name:lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate
CAS No.:1428847-46-4
Molecular Formula:C₁₉H₂₈N₃O₅S*Li
Molecular Weight:417.455
Hs Code.:

Synonyms:lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

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Chemical Property of lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

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Technology Process of lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

There total 5 articles about lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428847-45-3
methyl 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)-methylsulfonamido)benzoate

: 1428847-46-4
lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 6h;

Reference yield:

: 1239278-73-9
3-cyclopropylmethoxy-4-methanesulfonylaminobenzoic acid methyl ester

: 1428847-46-4
lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 12 h / 110 °C / Microwave irradiation

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 20 °C

3: potassium carbonate / acetonitrile / 3 h / 130 °C / Microwave irradiation

4: water; lithium hydroxide / tetrahydrofuran / 6 h / 20 °C

With carbon tetrabromide; water; potassium carbonate; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 1428847-44-2
methyl 4-(N-(2-bromoethyl)methylsulfonamido)-3-(cyclopropylmethoxy)benzoate?

: 1428847-46-4
lithium 3-(cyclopropylmethoxy)-4-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 3 h / 130 °C / Microwave irradiation

2: water; lithium hydroxide / tetrahydrofuran / 6 h / 20 °C

With water; potassium carbonate; lithium hydroxide; In tetrahydrofuran; acetonitrile;