benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate

Base Information

Chemical Name:benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate
CAS No.:1268157-65-8
Molecular Formula:C₂₄H₃₉N₃O₄
Molecular Weight:433.591
Hs Code.:

Synonyms:benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate

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Chemical Property of benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate

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Technology Process of benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate

There total 1 articles about benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 65564-05-8
3-[(benzyloxycarbonyl)amino]propanal

: 886362-50-1
1-(2-amino-ethyl)-N-Boc-cyclohexylamine

: 1268157-65-8
benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 25 ℃; for 24h; Molecular sieve; Inert atmosphere;
DOI:10.1021/jm101478n

Reference yield: 97.0%

: 1268157-65-8
benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate

: 1268157-71-6
tert-butyl 1-{2-[(3-aminopropyl)amino]ethyl}cyclohexylcarbamate

Guidance literature:: With 20% palladium hydroxide on carbon; hydrogen; In methanol; at 20 ℃; for 48h; under 2327.23 - 2585.81 Torr;
DOI:10.1021/jm101478n

Reference yield:

: 1268157-65-8
benzyl 3-[(2-{1-[(tert-butoxycarbonyl)amino]cyclohexyl}ethyl)amino]propylcarbamate

: 1268157-72-7
tert-butyl 1-[2-(2-oxotetrahydropyrimidin-1(2H)-yl)ethyl]cyclohexylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 20% palladium hydroxide on carbon; hydrogen / methanol / 48 h / 20 °C / 2327.23 - 2585.81 Torr

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 48 h / 70 °C / Inert atmosphere

With 20% palladium hydroxide on carbon; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol;
DOI:10.1021/jm101478n