methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enyl carbonate

Base Information

Chemical Name:methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enyl carbonate
CAS No.:1025722-71-7
Molecular Formula:C₂₂H₃₃NO₅
Molecular Weight:391.508
Hs Code.:

Synonyms:methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enyl carbonate

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Chemical Property of methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enyl carbonate

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Technology Process of methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enyl carbonate

There total 1 articles about methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1025722-81-9
ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enoate

: 79-22-1
methyl chloroformate

: 1025722-71-7
methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enyl carbonate

Guidance literature:: ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enoate; With boron trifluoride diethyl etherate; diisobutylaluminium hydride; In dichloromethane; toluene; at 0 ℃; for 0.5h;

methyl chloroformate; With pyridine; dmap; In dichloromethane; at 0 ℃; for 1h; Further stages.;
DOI:10.1021/jo702318d

Reference yield: 90.0%

: 67-56-1
methanol

: 1025722-71-7
methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-butyl-5-phenylpent-2-enyl carbonate

: 201230-82-2
carbon monoxide

: 1025722-99-9
methyl (5S,3E)-5-[N-(tert-butoxycarbonyl)amino]-4-butyl-6-phenylhex-3-enoate

Guidance literature:: With triphenylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; at 50 ℃; for 12h; under 22502.3 Torr;
DOI:10.1021/jo702318d