triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane

Base Information

Chemical Name:triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane
CAS No.:904925-67-3
Molecular Formula:C₃₀H₄₈OSi
Molecular Weight:452.796
Hs Code.:

Synonyms:triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane

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Chemical Property of triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane

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Technology Process of triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane

There total 3 articles about triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 904925-63-9
(4-benzyloxy-3-isopropyl-phenyl)-(2,6-dimethyl-4-triisopropylsilanyloxy-phenyl)-methanol

: 904925-67-3
triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / H₂ / Pd/C / acetic acid; ethanol / 14 h / 20 °C / 760 Torr

2: 98 percent / K₂CO₃ / dimethylformamide / 2 h / 20 °C

3: PdCl₂(dppf) / diethyl ether / 35 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; hydrogen; potassium carbonate; palladium on activated charcoal; In diethyl ether; ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ja060760v

Reference yield:

: 904925-65-1
trifluoro-methanesulfonic acid 4-(2,6-dimethyl-4-triisopropylsilanyloxy-benzyl)-2-isopropyl-phenyl ester

: 2234-82-4
1-propylmagnesium chloride

: 904925-67-3
triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In diethyl ether; at 35 ℃;
DOI:10.1021/ja060760v

Reference yield:

: 904925-64-0
4-(2,6-dimethyl-4-triisopropylsilanyloxy-benzyl)-2-isopropyl-phenol

: 904925-67-3
triisopropyl-[4-(3-isopropyl-4-propyl-benzyl)-3,5-dimethyl-phenoxy]-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃ / dimethylformamide / 2 h / 20 °C

2: PdCl₂(dppf) / diethyl ether / 35 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ja060760v