3-amino N,N-dimethyl 4-nitro aniline

Base Information

• Chemical Name: 3-amino N,N-dimethyl 4-nitro aniline
• CAS No.: 20691-71-8
• Molecular Formula: C8H11 N3 O2
• Molecular Weight: 181.194
• Hs Code.: 2921590090
• Mol file: 20691-71-8.mol

Synonyms:m-Phenylenediamine,N1,N1-dimethyl-4-nitro- (8CI); (3-Amino-4-nitrophenyl)dimethylamine;5-Dimethylamino-2-nitroaniline

Chemical Property of 3-amino N,N-dimethyl 4-nitro aniline

Chemical Property:

• Melting Point: 140℃
• Boiling Point: 355℃
• PKA: 0.75±0.22(Predicted)
• Flash Point: 168℃
• PSA: 75.08000
• Density: 1.280
• LogP: 2.34740
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

N1,N1-Dimethyl-4-nitrobenzene-1,3-diamine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-amino N,N-dimethyl 4-nitro aniline

There total 15 articles about 3-amino N,N-dimethyl 4-nitro aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

5-(N,N-dimethylamino)-2-nitroacetamide (129195-09-1) → 5-(dimethylamino)-2-nitroaniline (20691-71-8)

Guidance literature:

With sodium carbonate; at 50 ℃; for 8h;

DOI:10.1139/v93-159

Reference yield: 99.0%

5-chloro-2-nitroaniline (1635-61-6) + dimethyl amine (124-40-3) → 5-(dimethylamino)-2-nitroaniline (20691-71-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 150 ℃; for 12h;

DOI:10.1016/j.crci.2019.05.003

Reference yield: 97.0%

5-chloro-2-nitroaniline (1635-61-6) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 5-(dimethylamino)-2-nitroaniline (20691-71-8)

Guidance literature:

With potassium carbonate; 6-aminohexanoic acid; for 25h; Heating;

upstream raw materials:

N,N-dimethyl-3,4-dinitroaniline

5-bromo-2-nitroaniline

N,N-dimethylammonium chloride

5-fluoro-2-nitroaniline

Downstream raw materials:

4-dimethylamino-2-(phenylamino)nitrobenzene

5-(N,N-dimethylamino)-2-nitroacetamide

3-chloro-4-nitro-N,N-dimethylaniline

N⁴,N⁴-dimethyl-1,2,4-benzenetriamine