(2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine

Base Information

• Chemical Name: (2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine
• CAS No.: 402858-24-6
• Molecular Formula: C₂₀H₂₉NO₂
• Molecular Weight: 315.456

Synonyms:(2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine

Chemical Property of (2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine

Chemical Property:

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Technology Process of (2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine

There total 1 articles about (2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(E)-3-(2-methoxyphenyl)propenal (60125-24-8) + (-)-aminomenthol (55179-51-6) → (2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine (402858-24-6)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/ja002864q

Reference yield: 98.0%

methanol (67-56-1) + Phenylselenyl chloride (5707-04-0) + (2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine (402858-24-6) → (2S,4aS,7R,8aR)-2-[(1R,2R)-2-methoxy-2-(2-methoxy-phenyl)-1-phenylselenyl-ethyl]-4,4,7-trimethyl-octahydro-benzo[e][1,3]oxazine (882302-40-1)

Guidance literature:

In dichloromethane; at -15 ℃; for 24h;

DOI:10.1021/jo052582e

Reference yield: 92.0%

(2S,7R,9R,10S)-2-[2'-(o-methoxyphenyl)vinyl]-4,4,7-trimethyl-octahydro-2H-1,3-benzoxazine (402858-24-6) → (1R,2S,5R)-2-[1-[3-(2-methoxyphenyl)-allylamino]-1-methyl-ethyl]-5-methylcyclohexanol (906107-09-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 20 ℃;

DOI:10.1021/ja002864q

upstream raw materials:

(E)-3-(2-methoxyphenyl)propenal

(-)-aminomenthol

Downstream raw materials:

(1R,2S,5R)-2-[1-[3-(2-methoxyphenyl)-allylamino]-1-methyl-ethyl]-5-methylcyclohexanol

N-acryloyl-2α-[2-trans-(2'-methoxyphenyl)ethenyl]-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

(2S,4aS,7R,8aR)-2-[(1R,2R)-2-methoxy-2-(2-methoxy-phenyl)-1-phenylselenyl-ethyl]-4,4,7-trimethyl-octahydro-benzo[e][1,3]oxazine

(3aR,9aR)-N-(8-mentholyl)-5-methoxy-3a,4,9,9a-tetrahydrobenz[f]isoindoline

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