Trimethylsilyl-2,3,4,6-tetra-O-benzyl-b-D-glucopyranoside

Base Information

Chemical Name:Trimethylsilyl-2,3,4,6-tetra-O-benzyl-b-D-glucopyranoside
CAS No.:80312-55-6
Molecular Formula:C₃₇H₄₄O₆Si
Molecular Weight:612.838
Hs Code.:
European Community (EC) Number:618-307-9
DSSTox Substance ID:DTXSID001149633
Nikkaji Number:J597.210H
Mol file:80312-55-6.mol

Synonyms:Trimethylsilyl-2,3,4,6-tetra-O-benzyl-b-D-glucopyranoside;89825-08-1;80312-55-6;SCHEMBL7103873;DTXSID001149633;2,3,4,6-Tetrakis-O-(phenylmethyl)-1-O-(trimethylsilyl)-beta-D-glucopyranose

Suppliers and Price of Trimethylsilyl-2,3,4,6-tetra-O-benzyl-b-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Trimethylsilyl-2,3,4,6-tetra-O-benzyl-b-D-glucopyranoside

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:15
Exact Mass:612.29071565
Heavy Atom Count:44
Complexity:766

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Si](C)(C)OC1C(C(C(C(O1)COCC2=CC=CC=C2)OCC3=CC=CC=C3)OCC4=CC=CC=C4)OCC5=CC=CC=C5
Isomeric SMILES:C[Si](C)(C)O[C@H]1[C@@H]([C@H]([C@@H]([C@H](O1)COCC2=CC=CC=C2)OCC3=CC=CC=C3)OCC4=CC=CC=C4)OCC5=CC=CC=C5

Technology Process of Trimethylsilyl-2,3,4,6-tetra-O-benzyl-b-D-glucopyranoside

There total 3 articles about Trimethylsilyl-2,3,4,6-tetra-O-benzyl-b-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 75-77-4
chloro-trimethyl-silane

: 6564-72-3
2,3,4,6-tetra-O-benzyl-D-glucopyranose

: 80312-55-6
1-O-trimethylsilyl-2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: With triethylamine; In benzene; for 2h; Heating;
DOI:10.1055/s-1982-30012

Reference yield:

: 2083-91-2
N,N-Dimethyltrimethylsilylamine

: 6386-24-9
2,3,4,6-tetra-O-benzyl-D-galactopyranose

: 30608-21-0,80312-55-6,85982-86-1,85982-87-2,85982-88-3,85982-89-4,89825-08-1
2,3,4,6-tetra-O-benzyl-1-O-trimethylsilyl-α,β-D-galactopyranose

Guidance literature:: In dichloromethane; at -40 ℃; for 21h; Inert atmosphere;
DOI:10.1016/j.carres.2019.01.013

Reference yield:

: 1450-14-2
1,1,1,2,2,2-hexamethyldisilane

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 30608-21-0
1-O-trimethylsilyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

: 80312-55-6
1-O-trimethylsilyl-2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In N,N-dimethyl acetamide; at 80 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1039/b608958e