(Z)-2-(1-benzyl-2-(4-chlorophenyl)-1H-indol-3-yl)-1-phenylvinyl benzoate

Base Information

Chemical Name:(Z)-2-(1-benzyl-2-(4-chlorophenyl)-1H-indol-3-yl)-1-phenylvinyl benzoate
CAS No.:1393131-27-5
Molecular Formula:C₃₆H₂₆ClNO₂
Molecular Weight:540.061
Hs Code.:

Synonyms:(Z)-2-(1-benzyl-2-(4-chlorophenyl)-1H-indol-3-yl)-1-phenylvinyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(1-benzyl-2-(4-chlorophenyl)-1H-indol-3-yl)-1-phenylvinyl benzoate

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Technology Process of (Z)-2-(1-benzyl-2-(4-chlorophenyl)-1H-indol-3-yl)-1-phenylvinyl benzoate

There total 2 articles about (Z)-2-(1-benzyl-2-(4-chlorophenyl)-1H-indol-3-yl)-1-phenylvinyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1393131-10-6
N-benzyl-4-chloro-N-(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)benzamide

: 98-88-4
benzoyl chloride

: 1393131-27-5
(Z)-2-(1-benzyl-2-(4-chlorophenyl)-1H-indol-3-yl)-1-phenylvinyl benzoate

Guidance literature:: With tributylphosphine; triethylamine; In dichloromethane; at 20 ℃; for 2h; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c2cc33972b

Reference yield:

: 1309272-98-7
N-benzyl-4-chloro-N-(2-formylphenyl)benzamide

: 98-86-2
acetophenone

: 1393131-27-5
(Z)-2-(1-benzyl-2-(4-chlorophenyl)-1H-indol-3-yl)-1-phenylvinyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 12 h / 20 °C / Inert atmosphere

2: tributylphosphine; triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With tributylphosphine; sodium methylate; triethylamine; In methanol; dichloromethane; 2: Wittig reaction;
DOI:10.1039/c2cc33972b