3-Chloro-2,2,3,3-tetraphenylpropanenitrile

Base Information

• Chemical Name: 3-Chloro-2,2,3,3-tetraphenylpropanenitrile
• CAS No.: 155801-34-6
• Molecular Formula: C₂₇H₂₀ClN
• Molecular Weight: 393.915

Synonyms:3-Chloro-2,2,3,3-tetraphenylpropanenitrile

Chemical Property of 3-Chloro-2,2,3,3-tetraphenylpropanenitrile

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 3-Chloro-2,2,3,3-tetraphenylpropanenitrile

There total 1 articles about 3-Chloro-2,2,3,3-tetraphenylpropanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

trimethylsilyl cyanide (7677-24-9) + 1,2-dichloro-1,1,2,2-tetraphenylethane (1600-30-2) → 3-Chloro-2,2,3,3-tetraphenylpropanenitrile (155801-34-6)

Guidance literature:

With titanium tetrachloride; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1021/jo00093a016

Reference yield: 98.0%

methanol (67-56-1) + 3-Chloro-2,2,3,3-tetraphenylpropanenitrile (155801-34-6) → 3-Methoxy-2,2,3,3-tetraphenylpropanenitrile

Guidance literature:

With silver trifluoroacetate; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1021/jo00123a032

Reference yield: 90.0%

trimethylsilyl cyanide (7677-24-9) + 3-Chloro-2,2,3,3-tetraphenylpropanenitrile (155801-34-6) → 2,2,3,3-tetraphenylsuccinonitrile (3122-21-2)

Guidance literature:

With titanium tetrachloride; In dichloromethane; 1.) 0 deg C, 2.0 h, 2.) r.t., 2.5 h;

DOI:10.1021/jo00093a016

upstream raw materials:

trimethylsilyl cyanide

1,2-dichloro-1,1,2,2-tetraphenylethane

Downstream raw materials:

2,2,3,3-tetraphenylsuccinonitrile

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