2,4,6-trimethoxybenzyl phenyl sulfide

Base Information

• Chemical Name: 2,4,6-trimethoxybenzyl phenyl sulfide
• CAS No.: 197142-05-5
• Molecular Formula: C₁₆H₁₈O₃S
• Molecular Weight: 290.383
• Mol file: 197142-05-5.mol

Synonyms:2,4,6-trimethoxybenzyl phenyl sulfide

Chemical Property of 2,4,6-trimethoxybenzyl phenyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,6-trimethoxybenzyl phenyl sulfide

There total 2 articles about 2,4,6-trimethoxybenzyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-trimethoxybenzaldehyde (830-79-5) → 2,4,6-trimethoxybenzyl phenyl sulfide (197142-05-5)

Guidance literature:

Multi-step reaction with 2 steps

1: NaBH₄

2: TsOH / benzene

With sodium tetrahydroborate; toluene-4-sulfonic acid; In benzene;

DOI:10.1016/S0040-4020(97)00560-7

Reference yield:

2,4,6-trimethoxybenzyl alcohol (61040-78-6) + thiophenol (108-98-5) → 2,4,6-trimethoxybenzyl phenyl sulfide (197142-05-5)

Guidance literature:

With toluene-4-sulfonic acid; In benzene;

DOI:10.1016/S0040-4020(97)00560-7

Reference yield:

potassium acetate (127-08-2) + 2,4,6-trimethoxybenzyl phenyl sulfide (197142-05-5) → 2,4,6-trimethoxybenzaldehyde (830-79-5) + 2,4,6-trimethoxybenzyl alcohol (61040-78-6) + diphenyldisulfane (882-33-7) + 2,4,6-trimethoxybenzyl acetate (149286-58-8)

Guidance literature:

With Co(III)W; In water; acetic acid; for 0.5h; Product distribution; Ambient temperature;

DOI:10.1016/S0040-4020(97)00560-7

upstream raw materials:

2,4,6-trimethoxybenzyl alcohol

thiophenol

2,4,6-trimethoxybenzaldehyde

Downstream raw materials:

2,4,6-trimethoxybenzaldehyde

2,4,6-trimethoxybenzyl alcohol

diphenyldisulfane

2,4,6-trimethoxybenzyl acetate