3--5-(hydroxymethyl)-6H-1,4,2-dioxazine

Base Information

Chemical Name:3--5-(hydroxymethyl)-6H-1,4,2-dioxazine
CAS No.:80041-92-5
Molecular Formula:C₁₂H₁₃NO₅
Molecular Weight:251.239
Hs Code.:

3-<o-(carbomethoxy)phenyl>-5-(hydroxymethyl)-6H-1,4,2-dioxazine

Synonyms:3--5-(hydroxymethyl)-6H-1,4,2-dioxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3--5-(hydroxymethyl)-6H-1,4,2-dioxazine

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Technology Process of 3--5-(hydroxymethyl)-6H-1,4,2-dioxazine

There total 2 articles about 3--5-(hydroxymethyl)-6H-1,4,2-dioxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 80041-90-3
N-<(2,3-epoxypropyl)oxy>phthalimide

: 80041-92-5
3--5-(hydroxymethyl)-6H-1,4,2-dioxazine

Guidance literature:: With tert-butylamine; for 1h;
DOI:10.1021/jo00342a029

Reference yield:

: 524-38-9
N-hydroxyphthalimide

: 80041-92-5
3--5-(hydroxymethyl)-6H-1,4,2-dioxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / Et₃N / dimethylformamide / 12 h

2: 100 percent / t-BuNH₂ / 1 h

With tert-butylamine; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jo00342a029