2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester

Base Information

Chemical Name:2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester
CAS No.:941594-46-3
Molecular Formula:C₂₂H₂₅NO₇
Molecular Weight:415.443
Hs Code.:

Synonyms:2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester

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Chemical Property of 2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester

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Technology Process of 2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester

There total 3 articles about 2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32864-38-3
tert-Butyl ethyl malonate

: 129464-01-3
2-(benzyloxy)-4-fluoro-1-nitrobenzene

: 941594-46-3
2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester

Guidance literature:: tert-Butyl ethyl malonate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 2h;

2-(benzyloxy)-4-fluoro-1-nitrobenzene; In N,N-dimethyl-formamide; at 50 ℃; for 7.5h;

Reference yield:

: 446-36-6
5-fluoro-2-nitrophenol

: 941594-46-3
2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 °C

2.2: 7.5 h / 50 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 941594-46-3
2-(3-benzyloxy-4-nitro-phenyl)-malonic acid tert-butyl ester ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 °C

2.2: 7.5 h / 50 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;