N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

Base Information

Chemical Name:N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide
CAS No.:1315330-96-1
Molecular Formula:C₇₀H₈₆N₂O₆
Molecular Weight:1051.46
Hs Code.:

Synonyms:N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

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Chemical Property of N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

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Technology Process of N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

There total 3 articles about N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 23708-56-7
6-undecanol

: 331861-94-0
1,7-dibromo-N,N'-bis(2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic acid diimide

: 1315330-96-1
N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 4h;
DOI:10.1016/j.dyepig.2011.03.022

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1315330-96-1
N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; bromine; iodine / 10 h / 85 °C

2: propionic acid / 26 h / 130 °C

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

With sulfuric acid; bromine; iodine; potassium carbonate; propionic acid; In N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2011.03.022

Reference yield:

: 927-49-1
dipentyl ketone

: 1315330-96-1
N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 1 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

With sodium tetrahydroborate; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2011.03.022