7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:1192261-23-6
Molecular Formula:C₇₅H₈₆O₁₅
Molecular Weight:1227.5
Hs Code.:

Synonyms:7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of 7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of 7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about 7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1229735-32-3
C₈₀H₉₄O₁₆

: 1192261-23-6
7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: C₈₀H₉₄O₁₆; With methanol; lithium methanolate; for 120h; Reflux;

With Amberlite IR 120 (H⁺); In methanol; at 20 ℃;
DOI:10.1071/CH09058

Reference yield: 70.0%

: 1192261-23-6
7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 83025-11-0
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl trichloroacetimidate

: 507-09-5
tiolacetic acid

: 1192261-24-7
7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: 7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside; 3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -10 ℃; Molecular sieve;

tiolacetic acid; With pyridine; In diethyl ether; at 20 ℃; for 72h; stereoselective reaction;
DOI:10.1071/CH09058

Reference yield:

: 1192261-23-6
7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 74808-09-6,83441-60-5,90357-89-4,90358-01-3,103368-01-0,103368-04-3,103368-06-5,104048-30-8,104048-33-1,132201-75-3,132748-02-8,114743-70-3
2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl trichloroacetimidate

: 1192261-25-8
7-octen-1-yl 4-O-[4,6-O-benzylidene-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -10 ℃; stereoselective reaction; Molecular sieve;
DOI:10.1071/CH09058