7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:1192261-24-7
Molecular Formula:C₈₉H₁₀₅NO₂₃
Molecular Weight:1556.81
Hs Code.:

7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Synonyms:7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of 7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of 7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about 7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1192261-23-6
7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 83025-11-0
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl trichloroacetimidate

: 507-09-5
tiolacetic acid

: 1192261-24-7
7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: 7-octen-1-yl 4-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside; 3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -10 ℃; Molecular sieve;

tiolacetic acid; With pyridine; In diethyl ether; at 20 ℃; for 72h; stereoselective reaction;
DOI:10.1071/CH09058

Reference yield: 95.0%

: 1192261-24-7
7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1263279-11-3
C₈₃H₉₉NO₂₀

Guidance literature:: 7-octen-1-yl 4-O-[3-O-(2-N-acetyl-2-deoxy-3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside; With methanol; sodium methylate; at 20 ℃; for 2h;

With Amberlite IR 120 (H⁺); In methanol; at 20 ℃;
DOI:10.1071/CH09058