2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate

Base Information

Chemical Name:2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate
CAS No.:1352622-07-1
Molecular Formula:C₁₆H₁₅BrCl₃NO₄S
Molecular Weight:503.628
Hs Code.:

Synonyms:2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate

There total 4 articles about 2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1352621-99-8
1-bromo-2-(3-methoxyphenylamino)ethanesulfonic acid 2,4,6-trichlorophenyl ester

: 1352622-07-1
2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate

Guidance literature:: With sodium cyanoborohydride; acetic acid; In water; acetonitrile; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2011.10.093

Reference yield:

: 1352621-86-3
2,4,6-trichlorophenyl 1-bromoethenesulfonate

: 1352622-07-1
2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.17 h / 100 °C / Neat (no solvent)

2: sodium cyanoborohydride; acetic acid / water; acetonitrile / 12 h / 20 °C

With sodium cyanoborohydride; acetic acid; In water; acetonitrile; 1: Michael addition;
DOI:10.1016/j.tetlet.2011.10.093

Reference yield:

: 88-06-2,67471-29-8
2,4,6-Trichlorophenol

: 1352622-07-1
2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / -78 - 20 °C

2.1: 2,2'-azobis(isobutyronitrile); bromine / 1,2-dichloro-ethane / 3 h / Reflux

2.2: 1.08 h / -78 - 20 °C

3.1: 0.17 h / 100 °C / Neat (no solvent)

4.1: sodium cyanoborohydride; acetic acid / water; acetonitrile / 12 h / 20 °C

With 2,2'-azobis(isobutyronitrile); bromine; sodium cyanoborohydride; acetic acid; triethylamine; In dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; 3.1: Michael addition;
DOI:10.1016/j.tetlet.2011.10.093