3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester

Base Information

Chemical Name:3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester
CAS No.:437614-02-3
Molecular Formula:C₃₇H₂₉IO₆
Molecular Weight:696.538
Hs Code.:

Synonyms:3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester

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Chemical Property of 3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester

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Technology Process of 3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester

There total 11 articles about 3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 244608-10-4
3-Benzyloxy-4-iodo-5-(3-methoxy-2-vinyl-benzoyloxy)-benzoic acid benzyl ester

: 437614-02-3
3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: O₃ / CH₂Cl₂

1.2: Ph₃P / CH₂Cl₂

2.1: 462 mg / Et₃N / CH₂Cl₂ / 17 h

With ozone; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(02)00096-0

Reference yield:

: 303-38-8
2,3-Dihydroxybenzoic acid

: 437614-02-3
3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: K₂CO₃ / dimethylformamide

2: LiOH; H₂O / tetrahydrofuran

3: oxalyl chloride / CH₂Cl₂; dimethylformamide / 1 h

4: 100 percent / Et₃N / CH₂Cl₂ / 6.5 h

5: 86 percent / Ph₃P; C₂Cl₆; Et₃N / acetonitrile / 0.75 h

6: 100 percent / tetrahydrofuran / 18.5 h / 25 °C

7: 39 mg / aq. NaOH / methanol / 96 h / Heating

8: oxalyl chloride / CH₂Cl₂; dimethylformamide / 1 h

9: 462 mg / Et₃N / CH₂Cl₂ / 17 h

With lithium hydroxide; sodium hydroxide; oxalyl dichloride; hexachloroethane; water; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(02)00096-0

Reference yield:

: 74272-78-9
2,3-dibenzyloxybenzoic acid

: 437614-02-3
3-Benzyloxy-5-(3-benzyloxy-2-vinyl-benzoyloxy)-4-iodo-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: oxalyl chloride / CH₂Cl₂; dimethylformamide / 1 h

2: 100 percent / Et₃N / CH₂Cl₂ / 6.5 h

3: 86 percent / Ph₃P; C₂Cl₆; Et₃N / acetonitrile / 0.75 h

4: 100 percent / tetrahydrofuran / 18.5 h / 25 °C

5: 39 mg / aq. NaOH / methanol / 96 h / Heating

6: oxalyl chloride / CH₂Cl₂; dimethylformamide / 1 h

7: 462 mg / Et₃N / CH₂Cl₂ / 17 h

With sodium hydroxide; oxalyl dichloride; hexachloroethane; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(02)00096-0