(1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol

Base Information

Chemical Name:(1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol
CAS No.:94103-15-8
Molecular Formula:C₂₀H₃₂O₅S₂
Molecular Weight:416.603
Hs Code.:

Synonyms:(1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol

Chemical Property:

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Technology Process of (1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol

There total 1 articles about (1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 94103-14-7
3-O-benzyl-D-glucose diethyl dithioacetal

: 67-64-1
acetone

: 94103-15-8
(1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol

Guidance literature:: With copper(II) sulfate;
DOI:10.1039/c39840000835

Reference yield: 84.0%

: 94103-15-8
(1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol

: 74-95-3
1,1-dibromomethane

: 94119-39-8
(4R,5S,6R)-5-Benzyloxy-4-(bis-ethylsulfanyl-methyl)-6-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-[1,3]dioxane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In 1,4-dioxane;
DOI:10.1039/c39840000835

Reference yield:

: 94103-15-8
(1R,2S,3R)-2-Benzyloxy-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4,4-bis-ethylsulfanyl-butane-1,3-diol

: 119930-71-1
2,2-Dimethyl-propionic acid (4R,5R,6S)-5-(tert-butyl-diphenyl-silanyloxy)-6-(2,6-dioxo-piperidin-4-yl)-[1,3]dioxan-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 13 steps

1: 69 percent / NaOH, Bu₄NI / dioxane; H₂O

2: HgCl₂, HgO / acetonitrile; H₂O

3: 99 percent / benzene

4: tetrahydrofuran

5: CsF / acetonitrile

6: H₂O₂, KOH / aq. ethanol

7: sodium ethoxide / tetrahydrofuran

8: aq. HCl / tetrahydrofuran

9: sodium metaperiodate / methanol; H₂O

10: 89 percent / sodium borohydrate / ethanol

11: 92 percent / pyridine

12: 92 percent / H₂ / 10percent Pd-C / ethanol

13: 97 percent / 2,6-lutidine / CH₂Cl₂

With 2,6-dimethylpyridine; hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; sodium periodate; hydrogen; dihydrogen peroxide; sodium ethanolate; tetra-(n-butyl)ammonium iodide; cesium fluoride; mercury dichloride; mercury(II) oxide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; ethanol; dichloromethane; water; acetonitrile; benzene;
DOI:10.1016/0040-4039(88)85094-9