C₁₈H₁₅Cl₃O₆

Base Information

• Chemical Name: C₁₈H₁₅Cl₃O₆
• CAS No.: 1246431-54-8
• Molecular Formula: C₁₈H₁₅Cl₃O₆
• Molecular Weight: 433.673
• Mol file: 1246431-54-8.mol

Synonyms:C₁₈H₁₅Cl₃O₆

Chemical Property of C₁₈H₁₅Cl₃O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₁₈H₁₅Cl₃O₆

There total 3 articles about C₁₈H₁₅Cl₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C19H17Cl3O7 (1246431-52-6) → C18H15Cl3O6 (1246431-54-8)

Guidance literature:

Electrochemical reaction;

DOI:10.1002/ejoc.201301128

Reference yield:

(3,5-dichloro-4-hydroxyphenyl)acetic acid methyl ester (409366-27-4) → C18H15Cl3O6 (1246431-54-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Electrochemical reaction

2: Electrochemical reaction

DOI:10.1002/ejoc.201301128

Reference yield:

Methyl 4-hydroxyphenylacetate (14199-15-6) → C18H15Cl3O6 (1246431-54-8)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrabutyl-ammonium chloride; hydrogenchloride / water; acetonitrile / Electrochemical reaction

2: Electrochemical reaction

3: Electrochemical reaction

With hydrogenchloride; tetrabutyl-ammonium chloride; In water; acetonitrile;

DOI:10.1002/ejoc.201301128

upstream raw materials:

C₁₉H₁₇Cl₃O₇

(3,5-dichloro-4-hydroxyphenyl)acetic acid methyl ester

Methyl 4-hydroxyphenylacetate

Downstream raw materials:

2-{4-[5-(carboxymethyl)-2-methoxyphenoxy]phenyl}acetic acid

(+)-O-methylthalibrine

(S)-armepavine

armepavine

Refernces

• 1、 Kashiwagi, Tsuneo,Fuchigami, Toshio,Saito, Tsuyoshi,Nishiyama, Shigeru,Atobe, Mahito. "Sequential paired electrosynthesis of a diaryl ether derivative using an electrochemical microreactor". supporting information. p. 799 - 801. Retrieved 2014/06/23.