(5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane

Base Information

Chemical Name:(5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane
CAS No.:1227484-31-2
Molecular Formula:C₁₆H₂₇BrO₄Si
Molecular Weight:391.377
Hs Code.:

Synonyms:(5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane

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Technology Process of (5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane

There total 1 articles about (5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1227484-27-6
(5-bromo-2-methoxy-4-(methoxymethoxy)phenyl)methanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1227484-31-2
(5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.089

Reference yield: 85.0%

: 1227484-31-2
(5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1227484-32-3
5-((tert-butyldimethylsilyloxy)methyl)-4-methoxy-2-(methoxymethoxy)benzaldehyde

Guidance literature:: (5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.089

Reference yield: 72.0%

: 1227484-31-2
(5-bromo-2-methoxy-4-(methoxymethoxy)benzyloxy)(tert-butyl)dimethylsilane

: 681-94-7
ethyl 2-(tributylstannyl)acetate

: 1337973-19-9
ethyl (5-(tert-butyldimethylsilanyloxymethyl)-4-methoxy-2-methoxymethoxyphenyl)acetate

Guidance literature:: With dichlorobis(tri-O-tolylphosphine)palladium; zinc dibromide; In N,N-dimethyl-formamide; at 80 ℃; for 14h; Inert atmosphere;
DOI:10.1007/s12272-011-0805-9