methyl 3-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propylcarbonate

Base Information

Chemical Name:methyl 3-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propylcarbonate
CAS No.:1130490-97-9
Molecular Formula:C₁₇H₂₅BO₅
Molecular Weight:320.193
Hs Code.:

Synonyms:methyl 3-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propylcarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propylcarbonate

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Technology Process of methyl 3-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propylcarbonate

There total 2 articles about methyl 3-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propylcarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 85217-69-2,87802-71-9
cinnamyl methyl carbonate

: 73183-34-3
bis(pinacol)diborane

: 1130490-97-9
methyl 3-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propylcarbonate

Guidance literature:: bis(pinacol)diborane; With CuCl(SIMes); sodium t-butanolate; In tetrahydrofuran; for 0.166667h; Inert atmosphere;

cinnamyl methyl carbonate; With methanol; In tetrahydrofuran; at 22 ℃; for 0.333333h; regioselective reaction; Inert atmosphere;

Reference yield: 76.0%

: 67-56-1
methanol

: 87802-71-9,85217-69-2
(E)-methyl cinnamyl carbonate

: 73183-34-3
bis(pinacol)diborane

: 1130490-97-9
methyl 3-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propylcarbonate

Guidance literature:: With sodium t-butanolate; (1,3-dimesitylimidazolidin-2-yl)copper(I) chloride; In toluene; under N2; diborane reacted with alkene in toluene in presence of Cu complex (5 mol%), NaO-t-Bu and MeOH at 22°C for 20 min; detd. by (1)H NMR spectra;