ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate

Base Information

Chemical Name:ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate
CAS No.:1354975-96-4
Molecular Formula:C₂₄H₃₁N₅O₃
Molecular Weight:437.542
Hs Code.:

Synonyms:ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate

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Chemical Property of ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate

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Technology Process of ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate

There total 5 articles about ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1354975-95-3
ethyl 2-((4-methoxyphenyl)amino)-1H-imidazo[4,5-c]pyridine-6-carboxylate

: 5472-49-1
1-(3-chloropropyl)piperidine hydrochloride

: 1354975-96-4
ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 65 ℃; for 12h;

Reference yield:

: 1000783-10-7
ethyl 4-amino-5-nitropyridine-2-carboxylate

: 1354975-96-4
ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methylcyclohexene / palladium 10% on activated carbon / isopropyl alcohol / 12 h / 100 °C / Sealed tube

2: dicyclohexyl-carbodiimide / tetrahydrofuran / 12 h / 65 °C

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 65 °C

With 4-methylcyclohexene; potassium carbonate; dicyclohexyl-carbodiimide; palladium 10% on activated carbon; In tetrahydrofuran; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 1918-02-1
picloram

: 1354975-96-4
ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen; lithium hydroxide / palladium 10% on activated carbon / water / 16 h / 40 - 70 °C / 2327.23 Torr

1.2: pH 3

2.1: potassium nitrate; sulfuric acid / 2.33 h / 20 - 75 °C

2.2: 12 h / 60 °C / Cooling with ice

2.3: Cooling with ice

3.1: 4-methylcyclohexene / palladium 10% on activated carbon / isopropyl alcohol / 12 h / 100 °C / Sealed tube

4.1: dicyclohexyl-carbodiimide / tetrahydrofuran / 12 h / 65 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 65 °C

With 4-methylcyclohexene; sulfuric acid; hydrogen; potassium carbonate; potassium nitrate; dicyclohexyl-carbodiimide; lithium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; water; N,N-dimethyl-formamide; isopropyl alcohol;