2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid

Base Information

Chemical Name:2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid
CAS No.:1354975-97-5
Molecular Formula:C₂₂H₂₇N₅O₃
Molecular Weight:409.488
Hs Code.:

Synonyms:2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid

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Chemical Property of 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid

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Technology Process of 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid

There total 6 articles about 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1354975-96-4
ethyl 2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylate

: 1354975-97-5
2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid

Guidance literature:: With hydrogenchloride; water; at 70 ℃; for 12h;

Reference yield:

: 1000783-10-7
ethyl 4-amino-5-nitropyridine-2-carboxylate

: 1354975-97-5
2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 4-methylcyclohexene / palladium 10% on activated carbon / isopropyl alcohol / 12 h / 100 °C / Sealed tube

2: dicyclohexyl-carbodiimide / tetrahydrofuran / 12 h / 65 °C

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 65 °C

4: hydrogenchloride; water / 12 h / 70 °C

With hydrogenchloride; 4-methylcyclohexene; water; potassium carbonate; dicyclohexyl-carbodiimide; palladium 10% on activated carbon; In tetrahydrofuran; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 1918-02-1
picloram

: 1354975-97-5
2-((4-methoxyphenyl)amino)-1-(3-(piperidin-1-yl)propyl)-1H-imidazo[4,5-c]pyridine-6-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen; lithium hydroxide / palladium 10% on activated carbon / water / 16 h / 40 - 70 °C / 2327.23 Torr

1.2: pH 3

2.1: potassium nitrate; sulfuric acid / 2.33 h / 20 - 75 °C

2.2: 12 h / 60 °C / Cooling with ice

2.3: Cooling with ice

3.1: 4-methylcyclohexene / palladium 10% on activated carbon / isopropyl alcohol / 12 h / 100 °C / Sealed tube

4.1: dicyclohexyl-carbodiimide / tetrahydrofuran / 12 h / 65 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 65 °C

6.1: hydrogenchloride; water / 12 h / 70 °C

With hydrogenchloride; 4-methylcyclohexene; sulfuric acid; water; hydrogen; potassium carbonate; potassium nitrate; dicyclohexyl-carbodiimide; lithium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; water; N,N-dimethyl-formamide; isopropyl alcohol;