N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

Base Information

Chemical Name:N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide
CAS No.:330940-57-3
Molecular Formula:C₂₃H₁₉Cl₂N₅O₂
Molecular Weight:468.342
Hs Code.:

Synonyms:N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

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Chemical Property of N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

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Technology Process of N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

There total 5 articles about N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-{4-chloro-2-[N-(5-chloro(pyridin-2-yl))carbamoyl]phenyl}(4-cyanophenyl)carboxamide

: 109-81-9
N-methyl-ethane-1,2-diamine

: 330940-57-3
N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

Guidance literature:: N-{4-chloro-2-[N-(5-chloro(pyridin-2-yl))carbamoyl]phenyl}(4-cyanophenyl)carboxamide; With pyridine; hydrogen sulfide; triethylamine; at 0 - 20 ℃;

With methyl iodide; In acetone; for 2h; Reflux;

N-methyl-ethane-1,2-diamine; With acetic acid; In methanol; for 2h; Reflux;

Reference yield:

: 4743-17-3
5-Chloroisatoic anhydride

: 330940-57-3
N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

1.2: -78 - 20 °C

2.1: pyridine / dichloromethane / 20 °C

3.1: pyridine; triethylamine; hydrogen sulfide / 0 - 20 °C

3.2: 2 h / Reflux

3.3: 2 h / Reflux

With pyridine; hydrogen sulfide; potassium hexamethylsilazane; triethylamine; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 1072-98-6
5-chloro-2-pyridylamine

: 330940-57-3
N-{4-chloro-2-[N-(5-chloro(2-pyridyl))carbamoyl]phenyl}[4-(1-methyl(2-imidazolin-2-yl))phenyl]carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

1.2: -78 - 20 °C

2.1: pyridine / dichloromethane / 20 °C

3.1: pyridine; triethylamine; hydrogen sulfide / 0 - 20 °C

3.2: 2 h / Reflux

3.3: 2 h / Reflux

With pyridine; hydrogen sulfide; potassium hexamethylsilazane; triethylamine; In tetrahydrofuran; dichloromethane; toluene;