N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine

Base Information

Chemical Name:N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine
CAS No.:1149380-50-6
Molecular Formula:C₁₈H₁₈N₆O₂
Molecular Weight:350.38
Hs Code.:

Synonyms:N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine

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Chemical Property of N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine

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Technology Process of N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine

There total 7 articles about N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1149380-51-7
2-(3-(5-(chloromethyl)-1,2,4-oxadiazol-3-yl)phenyl)imidazo[1,2-b]pyridazine

: 109-85-3
2-methoxyethylamine

: 1149380-50-6
N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine

Guidance literature:: sodium iodide; In ethanol; for 2h; Heating / reflux;

Reference yield:

: 6136-68-1
3-acethylbenzonitrile

: 1149380-50-6
N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine

Guidance literature:: Multi-step reaction with 7 steps

1: bromine / diethyl ether / 4 h / 0 - 20 °C

2: ethanol / 10 h / Reflux

3: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 5 h / 20 °C

4: hydroxylamine hydrochloride; triethylamine / ethanol / 4 h / Reflux

5: toluene / 24 h / Reflux

6: toluene / 2 h / Reflux

7: sodium iodide / ethanol / 2 h / Reflux

With hydroxylamine hydrochloride; hydrogen; bromine; triethylamine; palladium 10% on activated carbon; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; ethanol; toluene;

Reference yield:

: 50916-55-7
3-(2-bromoacetyl)benzonitrile

: 1149380-50-6
N-((3-(3-(imidazo[1,2-b]pyridazin-2-yl)phenyl)-1,2,4-oxadiazol-5-yl)methyl)-2-methoxyethanamine

Guidance literature:: Multi-step reaction with 6 steps

1: ethanol / 10 h / Reflux

2: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 5 h / 20 °C

3: hydroxylamine hydrochloride; triethylamine / ethanol / 4 h / Reflux

4: toluene / 24 h / Reflux

5: toluene / 2 h / Reflux

6: sodium iodide / ethanol / 2 h / Reflux

With hydroxylamine hydrochloride; hydrogen; triethylamine; palladium 10% on activated carbon; sodium iodide; In tetrahydrofuran; methanol; ethanol; toluene;