3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime

Base Information

• Chemical Name: 3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime
• CAS No.: 184969-63-9
• Molecular Formula: C₂₉H₄₂Cl₂N₂O₃Si
• Molecular Weight: 565.656

Synonyms:3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime

Chemical Property of 3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime

Chemical Property:

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Technology Process of 3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime

There total 1 articles about 3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methoxylamine hydrochloride (593-56-6) + 3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethyl-ethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone (184969-61-7) → 3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime (184969-63-9)

Guidance literature:

With sodium acetate; In ethanol; water; at 20 ℃; for 12 - 18h;

Reference yield:

3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime (184969-63-9) → C23H28Cl2N2O3 (184969-64-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 2h;

Reference yield:

3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethylethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime (184969-63-9) + CH3 OH(NH3) → 3-(3,4-dichlorophenyl)-1-hydroxy-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone O-methyloxime

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; water; ethyl acetate;

upstream raw materials:

N-methoxylamine hydrochloride

3-(3,4-dichlorophenyl)-1-[[dimethyl(1,1-dimethyl-ethyl)silyl]oxy]-5-(4-hydroxy-4-phenyl-1-piperidinyl)-2-pentanone

Downstream raw materials:

C₂₃H₂₈Cl₂N₂O₃

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