methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate

Base Information

Chemical Name:methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate
CAS No.:1447047-16-6
Molecular Formula:C₄₂H₆₀N₆O₁₀
Molecular Weight:808.973
Hs Code.:

methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate

Synonyms:methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate

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Chemical Property of methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate

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Technology Process of methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate

There total 3 articles about methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1447047-13-3
tert-butyl (S)-2-((S)-2-(((benzyloxy)carbonyl)amino)-3-(4-(prop-2-yn-1-yloxy)phenyl)propanamido)-4-methylpentanoate

: 468065-37-4
methyl 6-azido-2-(boc-amino)hexanoate

: 1447047-16-6
methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 15h;
DOI:10.1002/chem.201204260

Reference yield:

: 21691-53-2
L-leucine tert-butyl ester

: 1447047-16-6
methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / dichloromethane; water / 15 h / 20 °C

With copper(ll) sulfate pentahydrate; benzotriazol-1-ol; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; water;
DOI:10.1002/chem.201204260

Reference yield:

: 1359969-23-5
(S)-2-(((benzyloxy)carbonyl)amino)-3-(4-(prop-2-yn-1-yloxy)phenyl)propanoic acid

: 1447047-16-6
methyl (S)-6-(4-((4-((S)-2-(((benzyloxy)carbonyl)amino)-3-(((S)-1-(tert-butoxy)-4-methyl-1-oxopentan-2-yl)amino)-3-oxopropyl)phenoxy)methyl)-1H-1,2,3-triazol-1-yl)-2-((tert-butoxycarbonyl)amino)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / dichloromethane; water / 15 h / 20 °C

With copper(ll) sulfate pentahydrate; benzotriazol-1-ol; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; water;
DOI:10.1002/chem.201204260