2-(benzyloxy)-6-bromobenzyl alcohol

Base Information

Chemical Name:2-(benzyloxy)-6-bromobenzyl alcohol
CAS No.:1334396-16-5
Molecular Formula:C₁₄H₁₃BrO₂
Molecular Weight:293.16
Hs Code.:

Synonyms:2-(benzyloxy)-6-bromobenzyl alcohol

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Chemical Property of 2-(benzyloxy)-6-bromobenzyl alcohol

Chemical Property:

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Technology Process of 2-(benzyloxy)-6-bromobenzyl alcohol

There total 3 articles about 2-(benzyloxy)-6-bromobenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 206002-17-7
2-(benzyloxy)-6-bromobenzaldehyde

: 1334396-16-5
2-(benzyloxy)-6-bromobenzyl alcohol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1002/anie.201103117

Reference yield:

: 22532-61-2
2-bromo-6-hydroxybenzaldehyde

: 1334396-16-5
2-(benzyloxy)-6-bromobenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 0.25 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201103117

Reference yield:

: 100-39-0
benzyl bromide

: 1334396-16-5
2-(benzyloxy)-6-bromobenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 0.25 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201103117