benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate

Base Information

Chemical Name:benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate
CAS No.:1413936-79-4
Molecular Formula:C₁₉H₂₇NO₅
Molecular Weight:349.427
Hs Code.:

Synonyms:benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate

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Chemical Property of benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate

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Technology Process of benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate

There total 1 articles about benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 946682-30-0
2-(4-(tert-butoxycarbonylamino)tetrahydro-2H-pyran-4-yl)acetic acid

: 100-39-0
benzyl bromide

: 1413936-79-4
benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 3h; Reflux;
DOI:10.3762/bjoc.8.142

Reference yield: 100.0%

: 1413936-79-4
benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate

: 1413936-80-7
benzyl 2-(4-aminotetrahydro-2H-pyran-4-yl)acetate hydrochloride

Guidance literature:: benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

With hydrogenchloride; In diethyl ether;
DOI:10.3762/bjoc.8.142

Reference yield:

: 1413936-79-4
benzyl 2-(4-(tert-butoxycarbonylamino) tetrahydro-2H-pyran-4-yl)acetate

: 1413936-81-8
C₄₈H₅₇N₅O₉S

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.3762/bjoc.8.142